By V Kourganoff
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Refer to: Chem. , 108,1953y (1988)*. p. (NA); 1 H NMR*, IR*, UV*, MS*. wt. 22 Synthesis -Refer to: Chem. , 120, 204680c (1994). p. and Spectra (NA). wt. 22 Synthesis -Preparation by condensation of gallic acid with pyrogallol, *in the presence of zinc chloride at 120° (good yield)  or at 145° for 3 h  (Nencki reaction); *in the presence of zinc chloride and phosphorous oxychloride at 80° for 2 h, via Fries rearrangement . -Also refer to: [104, 376, 465, 801] and Chem. , 80, 103486u (1974); 89, 186079y (1978); 106, 207622g (1987); 107, 10926Op (1987); 109, 86223d (1988); 112, 104863f (1990); 125, 5333v (1996); 129, 88025c (1998).
Wt. 11 Synthesis -Obtained by chromic oxidation (CrO3) of 6,7-dichloro3-phenylbenzofuran, followed by saponification of obtained keto ester . p. 141°5; IR . wt. t. for 20 min (98%) . p. 177° ; hemihydrate ; 1 H NMR . wt. 11 Syntheses -Preparation by adding aluminium chloride into a solution of 3,5-dichloro-2-hydroxybenzoyl chloride in benzene and heating at 60° for 3-4 h (60-70%) . -Also obtained by chromic oxidation (C1O3) of 5,7-dichloro3-phenylbenzofuran, followed by saponification of the obtained keto ester .
85, 116484v (1976)*; 90, 197343b (1979)*. p. (NA); 1 H NMR*, IR*, UV*, MS*. wt. 24 Synthesis -Preparation by treatment of 4-benzoyl-2,3-dihydrobenzoxazol-2-one (SM) with refluxing 20% hydrochloric acid for 10 h (68%). SM was obtained by UV light irradiation of N-benzoyl-2,3-dihydrobenzoxazol-2-one in acetonitrile for 48 h (21%) . p. 129°5-130°5 ; Spectra (NA). wt. 24 Synthesis -Refer to: . p. and Spectra (NA). wt. 24 Syntheses -Preparation by demethylation of 2-amino-5-methoxybenzophenone with boiling 48% hydrobromic acid , for 8 h (85%) .
Basic Methods in Transfer Problems by V Kourganoff